化工社化工社 化学情報印刷レポート · 研究参考用
Dimethyl Sulfide → Trimethylsulfonium Triflate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethyl Sulfide | HCID 1068 | — |
| 反応物 | Methyl triflate | HCID 9526 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Trimethylsulfonium Triflate | HCID 10933171 | — |
反応手順
16 mmol of dimethyl sulfide was dissolved in 10 ml of dichloromethane at 0° C., and about 17 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture to obtain a white solid product. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08536347B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-5cc9413dfef7447db1b13d03a866a5a8 |
| 出典メモ | uspto-grants-2013_09 |