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HRID 43293作成日:2026年10月23日

Dimethyl Sulfide → Trimethylsulfonium Triflate

https://huagongshe.com/ja/reaction/43293

反応式

関与物質

役割名称HCID仕込み量
反応物Dimethyl SulfideHCID 1068—
反応物Methyl triflateHCID 9526—
溶媒DichloromethaneHCID 6344—
生成物Trimethylsulfonium TriflateHCID 10933171—

反応手順

16 mmol of dimethyl sulfide was dissolved in 10 ml of dichloromethane at 0° C., and about 17 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture to obtain a white solid product. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08536347B2
出典データセットuspto-grants-2013_09
ORD IDord-5cc9413dfef7447db1b13d03a866a5a8
出典メモuspto-grants-2013_09