関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Octanoic Acid | HCID 379 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 生成物 | Octanoyl chloride | HCID 8124 | — |
反応手順
144.2 g of Octanoic Acid is charged at room temperature and heated to 40° C., then 154.64 g of Thionyl Chloride is added over a period of 1 hour and the reaction mixture is heated to reflux at 110° C. for 1½ hour to obtain crude Octanoyl Chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08536355B2 |
|---|
| 出典データセット | uspto-grants-2013_09 |
|---|
| ORD ID | ord-a167b60b59f440498a8198b5d77db73e |
|---|
| 出典メモ | uspto-grants-2013_09 |
|---|
