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Phenyl Salicylate → 2'-Ethyl-salicylanilide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenyl Salicylate | HCID 8361 | — |
| 反応物 | 2-Ethylaniline | HCID 11357 | — |
| 生成物 | 2'-Ethyl-salicylanilide | HCID 18760914 | — |
反応手順
The 2′-ethyl-salicylanilide was prepared by condensing phenyl salicylate with 2-ethylaniline then purified as described in Example 2a. The ligand mixture was then prepared from 2′-ethyl-salicylanilide and 1,1′-bi-2-naphthol using the procedure described in Example 2a. 31P NMR (121.77 MHz): several peaks between 117.1-118.8 ppm.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06664427B1 |
| 出典データセット | uspto-grants-2003_12 |
| ORD ID | ord-4bbf13c0bf514f11b9c4464537d267e6 |
| 出典メモ | uspto-grants-2003_12 |