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HRID 433462作成日：2026年10月25日

3,4-Dichloroaniline → N-(3,4-dichlorophenyl)alanine Benzyl Ester

https://huagongshe.com/reaction/433462

反応式

関与物質

役割名称HCID仕込み量
反応物3,4-DichloroanilineHCID 7257—
反応物Benzyl 2-oxopropanoateHCID 11769098—
生成物N-(3,4-dichlorophenyl)alanine Benzyl EsterHCID 15434839—

反応手順

Following General Procedure AA above and using 3,4-dichloroaniline (Aldrich) and benzyl pyruvate (prepared by following General Procedure AO above using benzyl alcohol in place of iso-butanol), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.4 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06667305B1
出典データセットuspto-grants-2003_12
ORD IDord-3214d454565642928b5ba0bc0bfa1cdd
出典メモuspto-grants-2003_12