化工社化工社 化学情報印刷レポート · 研究参考用
tert-Butyl bromoacetate → N-(3,4-dichlorophenyl)alanine Tert-butyloxycarbonylmethyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | tert-Butyl bromoacetate | HCID 79177 | — |
| 反応物 | N-(3,4-dichlorophenyl)alanine | HCID 5491659 | — |
| 生成物 | N-(3,4-dichlorophenyl)alanine Tert-butyloxycarbonylmethyl Ester | HCID 54406316 | — |
反応手順
Following General Procedure AE above and using N-(3,4-dichlorophenyl)alanine (from Example AB above) and tert-butyl bromoacetate (Aldrich), the title compound was prepared as a solid. The reaction was monitored by silica gel tlc (Rf=0.57 in 25% EtOAc/hexanes). Purification was by recrystallization from ethanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06667305B1 |
| 出典データセット | uspto-grants-2003_12 |
| ORD ID | ord-46b88333463f4c1eb863f4c4af99c8bb |
| 出典メモ | uspto-grants-2003_12 |