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Cadmium chloride, dihydrate → 5-Chloro-2-methyl-3-isothiazolone cadmium(II)chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cadmium chloride, dihydrate | HCID 24633 | — |
| 反応物 | 5-Chloro-2-methyl-4-isothiazolin-3-one | HCID 33344 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 5-Chloro-2-methyl-3-isothiazolone cadmium(II)chloride | HCID 86736469 | 200.3% |
反応手順
To a solution of 5.5 g (0.03 mole) of anhydrous cadmium chloride in 120 ml of ethanol was added a solution of 4.5 g (0.03 mole) of 5-chloro-2-methyl-3-isothiazolone in 25 ml of ethanol. A white precipitate formed immediately. The mixture was filtered and air dried to yield 10.0 g (100%) of product, m.p. >250° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04396413 |
| 出典データセット | uspto-grants-1983_08 |
| ORD ID | ord-241ae64773394f13b9e7dc796654469b |
| 出典メモ | uspto-grants-1983_08 |