Ethylamine → 2,2-Diethoxy-N-ethylethan-1-amine

HRID 434467

反応式

HRID 434467 の反応式
[CH2:1]([NH2:3])[CH3:2].Br[CH2:5][CH:6]([O:10][CH2:11][CH3:12])[O:7][CH2:8][CH3:9]>>[CH2:1]([NH:3][CH2:5][CH:6]([O:10][CH2:11][CH3:12])[O:7][CH2:8][CH3:9])[CH3:2]

参加物

3

反応物 2

HCID 6341EthylamineHCID 74852Ethane, 2-bromo-1,1-diethoxy-

生成物 1

HCID 125032612,2-Diethoxy-N-ethylethan-1-amine

実験手順

Ethylamine (38 grams) and 1-bromo-2,2-diethoxyethane (20 grams) were charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture was heated at reflux overnight. After this time the mixture was washed with aqueous sodium hydroxide and the organic phase separated from the aqueous phase. The organic phase was then distilled to yield the desired product N-ethyl-N-(2,2-diethoxyethyl)amine as an oil.

後処理

  1. customequipped with a mechanical stirrer
  2. temperaturethermometer and reflux condenser
  3. temperatureThe reaction mixture was heated
  4. temperatureat reflux overnight
  5. washAfter this time the mixture was washed with aqueous sodium hydroxide
  6. customthe organic phase separated from the aqueous phase
  7. distillationThe organic phase was then distilled

出典と根拠

ORDレコード
ord-8bfcf25171014b779da7e48d424b7a69
出典データセット
uspto-grants-1983_08
特許番号
US04397677

関連ノート

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