関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Boric Acid | HCID 7628 | — |
| 反応物 | Gluceptate Sodium | HCID 23664054 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | D-glycero-D-gulo-heptonic acid | HCID 25588 | — |
反応手順
The diboron ester of glucoheptonic acid was prepared as follows: Approximately 124 grams (2 mols) of boric acid and 248 grams (1 mol) of sodium glucoheptonate were charged to an esterification vessel containing about 600 milliliters of water as a solvent. With stirring, the temperature was maintained at about 25° C. for approximately 30 minutes. The mixture was thereafter diluted to a final volume of one liter with additional water.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04397812 |
|---|
| 出典データセット | uspto-grants-1983_08 |
|---|
| ORD ID | ord-14aa05a9e70445bf9970977a891a1384 |
|---|
| 出典メモ | uspto-grants-1983_08 |
|---|
