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O-Cresol → 2,6-Dimethylphenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | O-Cresol | HCID 335 | — |
| 反応物 | Phenol | HCID 996 | — |
| 反応物 | Dimethyl Ether | HCID 8254 | — |
| 反応物 | Silicon oxide (SiO) | HCID 66241 | — |
| 反応物 | Barium Oxide Nanoparticle Dispersion | HCID 9855530 | — |
| 触媒 | Ferrous oxide | HCID 449809 | — |
| 触媒 | HCID 178419084 | HCID 178419084 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 2,6-Dimethylphenol | HCID 11335 | — |
反応手順
A mixture of o-cresol and phenol, dimethyl ether and water in a molar ratio of 1:2:2.6 were reacted as described in Example 1. The catalyst contained iron oxide, vanadium oxide, silicon oxide and barium oxide in a molar ratio of 100:2:10:0.1. After working up, 2.6-xylenol was obtained with a selectivity of 99%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04400557 |
| 出典データセット | uspto-grants-1983_08 |
| ORD ID | ord-0e577805cbc34edb9d3509a4195c1f30 |
| 出典メモ | uspto-grants-1983_08 |