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Santonox → N-(1-methylethyl)-3-(3-chlorophenyl)-2-oxiranecarboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Santonox | HCID 7308 | — |
| 反応物 | m-Chloroperbenzoic acid | HCID 70297 | — |
| 反応物 | N-(1-Methylethyl)-3-Chlorocinnamoylcarboxamide | HCID 53986957 | — |
| 溶媒 | 1,2-Dichloroethane | HCID 11 | — |
| 生成物 | N-(1-methylethyl)-3-(3-chlorophenyl)-2-oxiranecarboxamide | HCID 13041335 | — |
反応手順
This compound was prepared from N-(1-methylethyl)-3-chlorocinnamoylcarboxamide (22.4 g.), m-chloroperbenzoic acid (23.6 g.), 4,4'-thiobis(6-tert-butyl-m-cresol) (0.3 g.), and ethylene dichloride as described in Example 7, and purified by recrystallization from ether. The compound melted at 131°-133°, and weighed 14.5 g.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04401832 |
| 出典データセット | uspto-grants-1983_08 |
| ORD ID | ord-d2d13e47b39349899f6b2d8a153831f9 |
| 出典メモ | uspto-grants-1983_08 |