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2-(Cyclohexylthio)-1H-isoindole-1,3(2H)-dione → Acetylcyclohexyl disulfide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(Cyclohexylthio)-1H-isoindole-1,3(2H)-dione | HCID 28777 | — |
| 反応物 | HCID 178418634 | HCID 178418634 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | Acetylcyclohexyl disulfide | HCID 88807735 | 98% |
反応手順
Thioacetic acid, 0.044 moles, 3.35 grams, is reacted with N-(cyclohexylthio)phthalimide in 100 ml of benzene and the product recovered following a procedure similar to Example 11. Acetylcyclohexyl disulfide, an amber oil, is recovered in 98% yield (7.5 grams). Analysis gives 51.27%C, 7.41%H and 31.78%S compared to 50.6%C, 7.38%H and 33.7%S calculated for C8H14OS2.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04006155 |
| 出典データセット | uspto-grants-1977_02 |
| ORD ID | ord-c03ecf6c99684936b0abe146aa4e1bb9 |
| 出典メモ | uspto-grants-1977_02 |