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Chlorotriethylsilane → 3-Triethylsilyl-2-oxazolidinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chlorotriethylsilane | HCID 13819 | — |
| 反応物 | 2-Oxazolidinone | HCID 73949 | — |
| 生成物 | 3-Triethylsilyl-2-oxazolidinone | HCID 21454776 | — |
反応手順
Following the previous example, but replacing the trimethylchlorosilane with triethylchlorosilane (63.3 g; 0.42 mol) and operating under similar conditions, the result is the compound of the above heading; a colourless fluid liquid, obtained with a similar yield. 2-oxazolidinone, calculated: 42.82%; found: 42.70%. Distils at 100° C between 2 and 4 mm.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04007168 |
| 出典データセット | uspto-grants-1977_02 |
| ORD ID | ord-ede3c3d0c1ca43f09684b307132c2b8e |
| 出典メモ | uspto-grants-1977_02 |