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Chloromethyl methyl sulfide → 2-Methyl-3-(((methylthio)methyl)thio)furan
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chloromethyl methyl sulfide | HCID 16916 | — |
| 反応物 | 2-Methyl-3-furanthiol | HCID 34286 | — |
| 反応物 | Sodium Methoxide | HCID 10942334 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 2-Methyl-3-(((methylthio)methyl)thio)furan | HCID 21503094 | — |
反応手順
Into a 25 ml round bottom flask equipped with magnetic stirrer, thermometer, water bath, and reflux condenser is added a solution containing 0.27 g of sodium methoxide (0.005 moles) in 3 ml. absolute methanol. While maintaining the solution at 25° C-30° C, 0.57 g (0.005 moles) of 2-methyl-3-furan thiol in 2 ml of absolute methanol is added thereto. At 25° C, 0.483 g (0.005 moles) of chloromethyl methyl sulfide having the formula:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04007287 |
| 出典データセット | uspto-grants-1977_02 |
| ORD ID | ord-3af128871d2f4be6bbc4f4e4581f0e8d |
| 出典メモ | uspto-grants-1977_02 |