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Potassium Hydroxide → HCID 21452975、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 1,8-Octanediamine | HCID 24250 | — |
| 反応物 | 4-(Trifluoromethoxy)benzoyl Chloride | HCID 142110 | — |
| 溶媒 | 1,2-Dichloroethane | HCID 11 | — |
| 生成物 | HCID 21452975 | HCID 21452975 | — |
反応手順
m.p. 164°-165° C., 12.0 g., was prepared as in Example 16 using 4-trifluoromethoxybenzoyl chloride (from 16.5 g. of 4-trifuoromethoxybenzoic acid as in Example 16) in 150 ml. of ethylene dichloride, 7.2 g. of 1,8-octanediamine, 200 ml. of 10% aqueous potassium hydroxide solution, 500 ml. of ethylene dichloride and recrystallization from methanol using decolorizing charcoal.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04009208 |
| 出典データセット | uspto-grants-1977_02 |
| ORD ID | ord-4328c9115ca741f790597127e260cedf |
| 出典メモ | uspto-grants-1977_02 |