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Benzoyl fluoride, 4-(trifluoromethoxy)- → N,N'-(1-Methylheptamethylene)bis(4-trifluoromethoxybenzamide)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzoyl fluoride, 4-(trifluoromethoxy)- | HCID 67612 | — |
| 反応物 | Octane-1,7-diamine | HCID 19967785 | — |
| 溶媒 | 1,2-Dichloroethane | HCID 11 | — |
| 生成物 | N,N'-(1-Methylheptamethylene)bis(4-trifluoromethoxybenzamide) | HCID 21452998 | — |
反応手順
m.p. 137°-138° C., 15.1 g., was prepared as in Example 20 using 18.7 g. of 4-trifluoromethoxybenzoyl fluoride in 50 ml. of ehtylene dichloride, 6.0 g. of 1,7-octanediamine in 100 ml. of ethylene dichloride, 13.8 g. of anhydrous potassium carbonate, and recrystallization from chloroform.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04009208 |
| 出典データセット | uspto-grants-1977_02 |
| ORD ID | ord-86f39d7689d2494182f97a30f64e1f83 |
| 出典メモ | uspto-grants-1977_02 |