化工社化工社 化学情報印刷レポート · 研究参考用
N,N-Dimethylallylamine → Allyl n-butoxymethyl dimethylammonium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N,N-Dimethylallylamine | HCID 75082 | — |
| 反応物 | 1-(Chloromethoxy)butane | HCID 11105357 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | Allyl n-butoxymethyl dimethylammonium chloride | HCID 21429949 | — |
反応手順
24.7 grams of chloromethyl butyl ether was added to 17 grams of allyl dimethylamine in 32 grams of ethyl acetate. The reaction was highly exothermic and two layers formed very rapidly. Stirring was continued at 25° C. for 24 hours, after which the solvent was removed by vacuum. Chloride analysis of the rather viscous liquid product indicated 91% of theoretical.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04029658 |
| 出典データセット | uspto-grants-1977_06 |
| ORD ID | ord-555e2f750b504c65a2b53b679bcae8c9 |
| 出典メモ | uspto-grants-1977_06 |