Hydroxylamine → HCID 23065677、化合物
反応式
C1(=O)CCCCC1.O=[C:9]1[CH2:14][CH2:13][CH2:12][CH2:11][CH:10]1[CH2:15][CH:16]1[CH2:21][CH2:20][CH2:19][CH2:18][C:17]1=O.[NH2:23]O>>[CH2:21]1[C:16]2[CH:17]([NH:23][CH:9]3[C:10]([CH:15]=2)=[CH:11][CH:12]=[CH:13][CH2:14]3)[CH2:18][CH2:19][CH2:20]1参加物
4
実験手順
Sym. octahydroacridine was prepared by converting cyclohexanone to di-(2-oxo-cyclohex-1-yl)-methane and further reacting with hydroxylamine according to the method of Gill et al (JACS 1952, 74, 4923) and was isolated as a colourless oil b.p. 110°-15°/0.5 mm. in 40% overall yield.
出典と根拠
- ORDレコード
- ord-3e4b6eb975ea4982a5ab2c1e96a3f3a8
- 出典データセット
- uspto-grants-1977_06
- 特許番号
- US04029668
反応ノート
読み込み中…