Tetrafluoro-m-phenylenediamine dihydrochloride → 4-Amino-1-[2-(2-naphthyl)ethyl]-piperidine
反応式
C([NH:9][CH:10]1[CH2:15][CH2:14][N:13]([CH2:16][CH2:17][C:18]2[CH:27]=[CH:26][C:25]3[C:20](=[CH:21][CH:22]=[CH:23][CH:24]=3)[CH:19]=2)[CH2:12][CH2:11]1)(=O)C1C=CC=CC=1.C1(N)C(F)=C(F)C(F)=C(N)C=1F.Cl.Cl>Cl>[NH2:9][CH:10]1[CH2:11][CH2:12][N:13]([CH2:16][CH2:17][C:18]2[CH:27]=[CH:26][C:25]3[C:20](=[CH:21][CH:22]=[CH:23][CH:24]=3)[CH:19]=2)[CH2:14][CH2:15]1参加物
4
実験手順
4-Benzamido-1-[2-(2-naphthyl)ethyl]piperidine (1.0 g.) was suspended in 6N HCl (40 ml.) and boiled for 96 hr. The resulting solution was worked up in the manner of Example 72 to give the title compound (0.558 g.) as the dihydrochloride, pale yellow needles, m.p. >300° (decomp.)
出典と根拠
- ORDレコード
- ord-4c8170c8499b46af9196e837392da24e
- 出典データセット
- uspto-grants-1977_06
- 特許番号
- US04029801
反応ノート
読み込み中…