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Lauric Acid → Silver laurate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Lauric Acid | HCID 3893 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Silver Nitrate | HCID 24470 | — |
| 溶媒 | Water | HCID 962 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Silver laurate | HCID 9904644 | — |
反応手順
1.9 g of sodium hydroxide was dissolved in 100 ml of water, with which 12 g of lauric acid in 100 ml of toluene was mixed to emulsify (at 25° C). An aqueous solution of 8.5 g of silver nitrate dissolved in 50 ml of water was, then, added to the above emulsion to result in a separation into a silver laurate-containing toluene phase and an aqueous phase. After removal of the aqueous phase, the toluene phase was dispersed into 200 ml of ethanol, and then, silver laurate was collected by centrifuging. 12 g of spindle-like silver laurate crystals of a longer diameter of about 3 μ was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04030931 |
| 出典データセット | uspto-grants-1977_06 |
| ORD ID | ord-d6b89e35ccf54dd48e695c5a31b1be27 |
| 出典メモ | uspto-grants-1977_06 |