関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Phosphoric Acid | HCID 1004 | — |
| 反応物 | Tetramethylammonium hydroxide | HCID 60966 | — |
| 反応物 | Titanium oxide (Ti3O) | HCID 162651 | — |
| 生成物 | Tetramethylammonium | HCID 6380 | — |
| 生成物 | Phosphoric acid, titanium(4+) salt (4:3) | HCID 159761 | — |
反応手順
0.05 mol of tetramethylammonium hydroxide (N(CH3)4OH) in aqueous solution was mixed with 0.15 mol of orthophosphoric acid (H3PO4). Then 0.05 mol of titanium dioxide in the anatase form (i.e., native TiO2) was added to the reaction mixture. After thorough mixing, the mixture was sealed inside a pressure reactor at 6~7 atm and heated in an oven at 180° C. for three days. After cooling, rinsing, filtration, and drying, a tetramethylammonium form of layered titanium phosphate (NMe4TP) was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05514490 |
|---|
| 出典データセット | uspto-grants-1996_05 |
|---|
| ORD ID | ord-ede9e910bc3d42f199ed34b2e7fb4ec1 |
|---|
| 出典メモ | uspto-grants-1996_05 |
|---|
