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5-Bromovanillin → N-(3-chlorophenyl)-2-cyano-3-(3-bromo-4-hydroxy-5-methoxyphenyl) propenamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Bromovanillin | HCID 18099 | — |
| 反応物 | N-(3-chlorophenyl)-2-cyanoacetamide | HCID 679494 | — |
| 生成物 | N-(3-chlorophenyl)-2-cyano-3-(3-bromo-4-hydroxy-5-methoxyphenyl) propenamide | HCID 53730904 | 65% |
反応手順
The reaction was performed in the same manner as in Example 1 with 5-bromovanillin (1.38 g, 5.97 mmol) and N-(3-chlorophenyl) cyanoacetamide (1.16 g, 5.97 mmol) to give the objective N-(3-chlorophenyl)-2-cyano-3-(3-bromo-4-hydroxy-5-methoxyphenyl) propenamide (1.58 g, 65% in yield).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05514711 |
| 出典データセット | uspto-grants-1996_05 |
| ORD ID | ord-4408703937e1495ea883d675cacea422 |
| 出典メモ | uspto-grants-1996_05 |