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3-Fluoro-4-hydroxy-5-methoxybenzaldehyde → HCID 54180841、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Fluoro-4-hydroxy-5-methoxybenzaldehyde | HCID 598452 | — |
| 反応物 | N-(3-chlorophenyl)-2-cyanoacetamide | HCID 679494 | — |
| 生成物 | HCID 54180841 | HCID 54180841 | 57% |
反応手順
The reaction was effected in the same manner as in Example 1 with 5-fluorovanillin (410 mg, 2.41 mmol) and N-(3-chlorophenyl) cyanoacetamide (469 mg, 2.41 mmol) to give the objective N-(3-chlorophenyl)-2-cyano-3-(3-fluoro-4-hydroxy-5-methoxyphenyl) propenamide (476 mg, 57% in yield) as yellow powders.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05514711 |
| 出典データセット | uspto-grants-1996_05 |
| ORD ID | ord-7fe3ff9d1db443bc88731c55ea01d699 |
| 出典メモ | uspto-grants-1996_05 |