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HRID 439794作成日:2026年10月26日

Methanol → Benzoic acid, 4-ethyl-, methyl ester

https://huagongshe.com/reaction/439794

反応式

関与物質

役割名称HCID仕込み量
反応物MethanolHCID 887—
反応物4-Ethylbenzoic AcidHCID 12086—
反応物Thionyl ChlorideHCID 24386—
生成物Benzoic acid, 4-ethyl-, methyl esterHCID 23827—

反応手順

A mixture of 4-ethylbenzoic acid (5.12 g), thionyl chloride (3.0 ml) and methanol (150 ml) was heated and refluxed. After 3 hours, the mixture was concentrated under reduced pressure to give methyl 4-ethylbenzoate (5.59 g). this product was used in the subsequent step without purification.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05516777
出典データセットuspto-grants-1996_05
ORD IDord-cfb03ca1633a47faa484d1cc6cde5262
出典メモuspto-grants-1996_05