化工社化工社 化学情報印刷レポート · 研究参考用
Methanol → Benzoic acid, 4-ethyl-, methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | 4-Ethylbenzoic Acid | HCID 12086 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 生成物 | Benzoic acid, 4-ethyl-, methyl ester | HCID 23827 | — |
反応手順
A mixture of 4-ethylbenzoic acid (5.12 g), thionyl chloride (3.0 ml) and methanol (150 ml) was heated and refluxed. After 3 hours, the mixture was concentrated under reduced pressure to give methyl 4-ethylbenzoate (5.59 g). this product was used in the subsequent step without purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05516777 |
| 出典データセット | uspto-grants-1996_05 |
| ORD ID | ord-cfb03ca1633a47faa484d1cc6cde5262 |
| 出典メモ | uspto-grants-1996_05 |