化工社化工社 化学情報印刷レポート · 研究参考用
2-Octanol → Propan-2-yl 2-dodecylbenzene-1-sulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Octanol | HCID 20083 | — |
| 反応物 | p-Toluenesulfonic acid 1-methylheptyl ester | HCID 3912199 | — |
| 反応物 | 2-Dodecylbenzene-1-sulfonyl chloride | HCID 20439001 | — |
| 生成物 | Propan-2-yl 2-dodecylbenzene-1-sulfonate | HCID 23368822 | 83% |
反応手順
In Example of preparation of material 15, 2-octanol was used in place of 2-propanol in Example of preparation of material 14. In Example of preparation of material 16, dodecylbenzene sulfonyl chloride was used in place of p-toluene sulfonyl chloride in Example of preparation of material 14. Other procedures were made in the same way as Example of preparation of material 14. In Example of preparation of material 15, 1-methylheptyl p-toluenesulfonate was obtained in the yield of 72% and, in Example of preparation of material 16, 1-methylethyl dodecylbenzene sulfonate was obtained in the yield of 83%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05516839 |
| 出典データセット | uspto-grants-1996_05 |
| ORD ID | ord-f32a2b5f3ca24126a670cd0dd0ccc874 |
| 出典メモ | uspto-grants-1996_05 |