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((4-(tert-Butyl)phenyl)ethynyl)trimethylsilane → Trimethylsilyl[4-(4-methylpentyl)]phenylethyne
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | ((4-(tert-Butyl)phenyl)ethynyl)trimethylsilane | HCID 14989664 | — |
| 反応物 | 4-(4-Methylpentyl)bromobenzene | HCID 22409093 | — |
| 生成物 | Trimethylsilyl[4-(4-methylpentyl)]phenylethyne | HCID 54327813 | — |
反応手順
Using the same general procedure as described for Compound 21, but using instead 4-(4-methylpentyl)bromobenzene (Compound 30), the title compound was synthesized as a colorless oil. PMR (CDCl3): & 0.32 (9H, s), 0.93 (6H, d, J-6.6 Hz), 1.18-1.29 (2H, m), 1.52-1.70 (3H, m), 2.58 (2H, t, J-7.7 Hz), 7.12 (2H, d, J-8.1 Hz), 7.43 (2H, d, J-8.1 Hz).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05516904 |
| 出典データセット | uspto-grants-1996_05 |
| ORD ID | ord-6530a09d05024e3ba8c72547979e750b |
| 出典メモ | uspto-grants-1996_05 |