化工社化工社 化学情報印刷レポート · 研究参考用
(+)-1-(4-Nitrophenyl)-3-acetyl-4-methyl-7,8-methylenedioxy-3,4-dihydro-5H-2,3-benzodiazepine → Gyki-53405
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (+)-1-(4-Nitrophenyl)-3-acetyl-4-methyl-7,8-methylenedioxy-3,4-dihydro-5H-2,3-benzodiazepine | HCID 9976222 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Gyki-53405 | HCID 126756 | — |
反応手順
The title compound was prepared from the compound of Example 126 using the process described in Example 128. Melting point 169°-172° C. [α]D =-321.34° (c=1, MeOH) Enantiomeric purity: >99%
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05519019 |
| 出典データセット | uspto-grants-1996_05 |
| ORD ID | ord-616fb46fb2d441f7a3d4b22a0ecf4205 |
| 出典メモ | uspto-grants-1996_05 |