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HRID 440951作成日:2026年10月26日

5-(1-Naphthyl)-4-pentyn-1-ol → 5-(Naphth-1-yl)pentanol

https://huagongshe.com/reaction/440951

反応式

関与物質

役割名称HCID仕込み量
反応物5-(1-Naphthyl)-4-pentyn-1-olHCID 19955557—
反応物HCID 178418361HCID 178418361—
触媒PalladiumHCID 23938—
溶媒EthanolHCID 702—
生成物5-(Naphth-1-yl)pentanolHCID 1035320093.3%

反応手順

A mixture of 3.5 grams (0.017 mole) of 5-(naphth-1-yl)-4-pentyn-1-ol and 0.5 gram (catalyst) of 10% palladium on carbon in 30 mL of ethanol was shaken in a Parr hydrogenator until the theoretical amount of hydrogen gas was taken up. The reaction mixture was filtered to remove the catalyst, and the filtrate was concentrated under reduced pressure, yielding 3.4 grams of 5-(naphth-1-yl)pentanol. The NMR spectrum was consistent with the proposed structure.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05521192
出典データセットuspto-grants-1996_05
ORD IDord-ccbb9eb492614f1abada5b33b9b272a6
出典メモuspto-grants-1996_05