化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → Diazene, (nitrophenyl)phenyl-, (E)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 2-Nitro-2'-hydroxy-3',5'-bis(tert-amyl)azobenzene | HCID 104111 | — |
| 生成物 | Diazene, (nitrophenyl)phenyl-, (E)- | HCID 142206 | — |
反応手順
The same procedure as described in Example 1 was carried out except that the 27.4 grams of 50% sodium hydroxide was used with 155 grams of 2'-hydroxy-3',5'-di-tert-amyl-2-nitroazobenzene to give a ratio of moles of alkali to moles of o-nitroazobenzene intermediate of 0.848/1 compared to the ratio of 0.42/1 employed in Example 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04041044 |
| 出典データセット | uspto-grants-1977_08 |
| ORD ID | ord-2d3d8654b82045978a53888e521b7675 |
| 出典メモ | uspto-grants-1977_08 |