化工社化工社 化学情報印刷レポート · 研究参考用
Oxygen → Diphenylformamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Oxygen | HCID 977 | — |
| 反応物 | Methyldiphenylamine | HCID 11098 | — |
| 生成物 | Diphenylformamide | HCID 69081 | 43.3% |
反応手順
By essentially the procedure of Example 1, a tube was charged with 40 g of methyldiphenylamine and 2.0 g CuCl2. 2H2O. The reaction was run at 115°-125° C. for 2 hr at 290-400 psi. About 0.1 mole of oxygen was injected incrementally. GC/MS analysis showed a 98.6% conversion of methyldiphenylamine and a 43.3% yield of diphenylformamide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04042621 |
| 出典データセット | uspto-grants-1977_08 |
| ORD ID | ord-9030a9fdf81e4b68b1daa6a663d70bb7 |
| 出典メモ | uspto-grants-1977_08 |