化工社化工社 化学情報印刷レポート · 研究参考用
1-Iodonaphthalene → 5-Methyl-1-(1-naphthyl)-2-(1H)-pyridone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Iodonaphthalene | HCID 7004 | — |
| 反応物 | Sodium Carbonate | HCID 10340 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 2-Hydroxy-5-methylpyridine | HCID 70482 | — |
| 生成物 | 5-Methyl-1-(1-naphthyl)-2-(1H)-pyridone | HCID 10198577 | 68% |
反応手順
5-Methyl-1-(1-naphthyl)-2-(1H)-pyridone is prepared by the reaction of 5-methyl-2 -(1H)-pyridone and α-iodonaphthalene following the procedure of Example 1 but substituting anhydrous sodium carbonate for the potassium carbonate; yield 68%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04042699 |
| 出典データセット | uspto-grants-1977_08 |
| ORD ID | ord-96bf359109cb483e9710fb3628c93d32 |
| 出典メモ | uspto-grants-1977_08 |