化工社化工社 化学情報印刷レポート · 研究参考用
5-Chloro-2-nitrobenzoic acid → 5-Chloro-2-nitrobenzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Chloro-2-nitrobenzoic acid | HCID 17286 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 生成物 | 5-Chloro-2-nitrobenzoyl chloride | HCID 2723685 | 98% |
反応手順
100.00 g (0.50 mol) of 5-chloro-2-nitrobenzoic acid were mixed with 72.20 g (0.61 mol) of thionyl chloride and the mixture was heated under reflux for 2 h. The excess thionyl chloride was removed in vacuo. 106.50 g (ca. 98%) of crude 5-chloro-2-nitro-benzoyl chloride were obtained as an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08541410B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-98241a4d407344f4a0ba01242af87eef |
| 出典メモ | uspto-grants-2013_09 |