化工社化工社 化学情報印刷レポート · 研究参考用
Acetic Acid → 2-nitroethyl Acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Benzene | HCID 241 | — |
| 反応物 | HCID 22056827 | HCID 22056827 | — |
| 触媒 | Sulfuric Acid | HCID 1118 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 2-nitroethyl Acetate | HCID 11815399 | — |
反応手順
64 g nitroethanol, 50 ml glacial acetic acid, 250 ml benzene and 5 drops conc. H2SO4 were refluxed, using a water separator for 8 hours; 12 ml of H2O were collected. The solution was evaporated and vacuum distilled (1mm at 60° C) yielding 89 g colorless nitroethylacetate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04044020 |
| 出典データセット | uspto-grants-1977_08 |
| ORD ID | ord-69984e74caad4c0abca1aeb28fb2ec24 |
| 出典メモ | uspto-grants-1977_08 |