化工社化工社 化学情報印刷レポート · 研究参考用
Water → 1-(Hydroxymethyl)cyclohexan-1-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | 1-(Aminomethyl)cyclohexan-1-ol | HCID 77614 | — |
| 生成物 | 1-(Hydroxymethyl)cyclohexan-1-ol | HCID 251259 | — |
反応手順
Compounds of this type may be prepared from isophorone utilizing the methods described in U.S. Pat. Nos. 3,270,044 and 3,352,913 to form an amino methyl cyclohexanol which is then reacted with a carboxylic acid in a fusion cook by heating stoichiometric quantities of the amine and the acid until molten and stirring the molten mixture with a nitrogen sweep to drive off water vapor. The progress of the reaction is stopped when an acid number just below theoretical is obtained. Similarly, the carboxylate derivative can be formed from a hydroxymethyl cyclohexanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04044033 |
| 出典データセット | uspto-grants-1977_08 |
| ORD ID | ord-bdd398d5c3704a7b95a78d2539cfe0b5 |
| 出典メモ | uspto-grants-1977_08 |