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HRID 442049作成日:2026年10月25日

Water → 1-(Hydroxymethyl)cyclohexan-1-ol

https://huagongshe.com/reaction/442049

反応式

関与物質

役割名称HCID仕込み量
反応物WaterHCID 962—
反応物1-(Aminomethyl)cyclohexan-1-olHCID 77614—
生成物1-(Hydroxymethyl)cyclohexan-1-olHCID 251259—

反応手順

Compounds of this type may be prepared from isophorone utilizing the methods described in U.S. Pat. Nos. 3,270,044 and 3,352,913 to form an amino methyl cyclohexanol which is then reacted with a carboxylic acid in a fusion cook by heating stoichiometric quantities of the amine and the acid until molten and stirring the molten mixture with a nitrogen sweep to drive off water vapor. The progress of the reaction is stopped when an acid number just below theoretical is obtained. Similarly, the carboxylate derivative can be formed from a hydroxymethyl cyclohexanol.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04044033
出典データセットuspto-grants-1977_08
ORD IDord-bdd398d5c3704a7b95a78d2539cfe0b5
出典メモuspto-grants-1977_08