化工社化工社 化学情報印刷レポート · 研究参考用
5-Methyl-2-nitrobenzoic acid → 5-Methyl-2-nitrobenzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Methyl-2-nitrobenzoic acid | HCID 18371 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 生成物 | 5-Methyl-2-nitrobenzoyl chloride | HCID 3016013 | — |
反応手順
A mixture of 5-methyl-2-nitrobenzoic acid (3.6 g, 19.87 mmol) and thionyl chloride (18 mL) was stirred under reflux for 20 hours then concentrated under reduced pressure to give 5-methyl-2-nitrobenzoyl chloride (3.77 g) which was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08541407B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-2380136c791e4cb694bce3db9ce279d8 |
| 出典メモ | uspto-grants-2013_09 |