関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Silver | HCID 23954 | — |
| 反応物 | Silver Nitrate | HCID 24470 | — |
| 反応物 | Silver bromide | HCID 66199 | — |
| 反応物 | Potassium Bromide | HCID 253877 | — |
| 反応物 | Silver bromide iodide | HCID 436885 | — |
| 反応物 | Sodium Behenate | HCID 23668838 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Silver behenate | HCID 164971 | — |
反応手順
A silver behenate dispersion was prepared as described for INVENTION EXAMPLE 1, except that the dispersing medium used was a solution of 29.4 g of gelatin (type 7598 from AGFA GELATINFABRIK vorm. KOEPFF & SOEHNE) in 731 mL of distilled water instead of 30 g of type 7598 gelatin in 750 mL of distilled water and in addition contained 18.7 g of a silver bromide-iodide emulsion with 0.7 g of gelatin and 5.03 g of silver bromide-iodide (consisting of 99.7 mol % of silver bromide and 0.3 mol % of silver iodide) with a particle size of 0.05 μm; the quantity of sodium behenate solution added was 358 mL instead of 374 mL; and the addition rate of said sodium behenate solution was 44.1 mL/min instead of 46.6 mL/min. 0.088 moles of sodium behenate were utilized in the reaction, but the quantity of silver nitrate used was not recorded. After the reaction was completed, the free silver ions present were converted into silver bromide by titrating the dispersion with a potassium bromide solution.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US05891616 |
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| 出典データセット | uspto-grants-1999_04 |
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| ORD ID | ord-0e8ee6a03a754c42a1bde9bb8475a85f |
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| 出典メモ | uspto-grants-1999_04 |
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