化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → 1-Triethoxysilylglycerol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Glycerol | HCID 753 | — |
| 反応物 | Dicyclohexylamine | HCID 7582 | — |
| 反応物 | Chlorosilane | HCID 61622 | — |
| 反応物 | Triethoxychlorosilane | HCID 78398 | — |
| 生成物 | 1-Triethoxysilylglycerol | HCID 54427112 | 90% |
反応手順
Glycerol (GL) was reacted with chlorotriethoxysilane (CTS) in a 1:1 ratio at 0° C. in a 50/50 mixture of ethanol/cyclomethicone, using a 1:1 ratio of dicyclohexylamine to chlorosilane as the HCl scavenger. The resulting product, 1-triethoxysilylglycerol, was obtained in 90% yield and was dissolved to a 10% by weight solution in a 50/50 by volume mixture of ethanol/cyclomethicone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05891914 |
| 出典データセット | uspto-grants-1999_04 |
| ORD ID | ord-34a137cec1d84963b67a4990cd97ac55 |
| 出典メモ | uspto-grants-1999_04 |