3-Phenylpropylamine → (3-Phenyl-n-propyl)aminosulfonylacetonitrile

反応式

[C:1]1([CH2:7][CH2:8][CH2:9][NH2:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:11]([CH2:13][S:14](Cl)(=[O:16])=[O:15])#[N:12].C(NS(CC#N)(=O)=O)C1C=CC=CC=1>>[C:1]1([CH2:7][CH2:8][CH2:9][NH:10][S:14]([CH2:13][C:11]#[N:12])(=[O:16])=[O:15])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

参加物

反応物 3

HCID 162593-Phenylpropylamine

HCID 13142426Cyanomethanesulfonyl chloride

HCID 15410493HCID 15410493、化合物

生成物 1

HCID 15410494(3-Phenyl-n-propyl)aminosulfonylacetonitrile

実験手順

N-3-Phenyl-n-propyl cyanomethylsulfonamide was prepared with 3-phenyl-n-propylamine and cyanomethylsulphonyl chloride under the similar conditions as decribed for N-benzyl cyanomethylsulfonamide (Part A, EXAMPLE 12).

出典と根拠

ORDレコード: ord-c6fc72ffb57b4274923b4e27769c00a4
出典データセット: uspto-grants-1999_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05891917

反応ノート

読み込み中…