4,4'-Dimethylbenzhydrol → N-Isopropyl-3-[bis(4-methylphenyl)methyl]indole-2-sulfonamide

HRID 442874

反応式

HRID 442874 の反応式
[CH3:1][C:2]1[CH:16]=[CH:15][C:5]([CH:6](O)[C:7]2[CH:12]=[CH:11][C:10]([CH3:13])=[CH:9][CH:8]=2)=[CH:4][CH:3]=1.[CH:17]([NH:20][S:21]([C:24]1[NH:25][C:26]2[C:31]([CH:32]=1)=[CH:30][CH:29]=[CH:28][CH:27]=2)(=[O:23])=[O:22])([CH3:19])[CH3:18]>>[CH:17]([NH:20][S:21]([C:24]1[NH:25][C:26]2[C:31]([C:32]=1[CH:6]([C:7]1[CH:12]=[CH:11][C:10]([CH3:13])=[CH:9][CH:8]=1)[C:5]1[CH:15]=[CH:16][C:2]([CH3:1])=[CH:3][CH:4]=1)=[CH:30][CH:29]=[CH:28][CH:27]=2)(=[O:23])=[O:22])([CH3:19])[CH3:18]

参加物

3

反応物 2

HCID 2793564,4'-DimethylbenzhydrolHCID 54122335N-isopropylindole-2-sulfonamide

生成物 1

HCID 67594248N-Isopropyl-3-[bis(4-methylphenyl)methyl]indole-2-sulfonamide収率 75%

実験手順

Substantially the same procedure as in Example 266 was repeated using 4,4'-dimethylbenzhydrol (0.96 g, 4.50 mmol) and N-isopropylindole-2-sulfonamide (1.00 g, 4.46 mmol) to give 1.44 g (yield: 75%) of the title compound.

出典と根拠

ORDレコード
ord-5c8f49ed37024195bfe647246bc80055
出典データセット
uspto-grants-1999_04
特許番号
US05891902

関連ノート

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