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Phenyl phenylglyoxylate → Phenyl 4-chlorobenzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenyl phenylglyoxylate | HCID 13975017 | — |
| 反応物 | 4-Chlorophenyl phenylglyoxylate | HCID 54442020 | — |
| 触媒 | Tetraphenylphosphonium Chloride | HCID 164911 | — |
| 溶媒 | Chloroform | HCID 6212 | — |
| 生成物 | Phenyl 4-chlorobenzoate | HCID 260766 | — |
反応手順
The decarbonylation reaction of Example 79 was repeated except that phenyl phenylglyoxylate (PPG) was replaced with 4-chlorophenyl phenylglyoxylate (4-CPPG), and that the amounts of tetraphenylphosphonium chloride and chloroform were changed as set forth in Table 13. The results are set forth in Table 13.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05892091 |
| 出典データセット | uspto-grants-1999_04 |
| ORD ID | ord-b4c01714edc043b29f69990524dc94d0 |
| 出典メモ | uspto-grants-1999_04 |