化工社化工社 化学情報印刷レポート · 研究参考用
Cumene → 1-Bromo-4-isopropylbenzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cumene | HCID 7406 | — |
| 反応物 | Bromine | HCID 24408 | — |
| 生成物 | 1-Bromo-4-isopropylbenzene | HCID 11462 | — |
反応手順
This example describes the reaction of cumene with liquid bromine to give 4-bromocumene. 10 g of cumene, 5 g of catalyst composite material, zeolite K-L and 2.14 ml bromine were mixed in a batch reactor. The reaction mixture was stirred and heated up to 70° C. After completion of the reaction, the mixture was let to cool to room temperature and analysed by gas-chromatography. The conversion of cumene and the selectivity for 4-bromocumene were found to be 10.7 wt. % and 78.8%, respectiveley.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05892138 |
| 出典データセット | uspto-grants-1999_04 |
| ORD ID | ord-124f5561d52b43c3b9a32bade2aacdf8 |
| 出典メモ | uspto-grants-1999_04 |