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Acetic Acid → 4-Chloro-1-naphthol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Hydrogen Bromide | HCID 260 | — |
| 反応物 | 1-Chloro-4-methoxynaphthalene | HCID 606038 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4-Chloro-1-naphthol | HCID 11787 | — |
反応手順
The known compound 1-chloro-4-methoxynaphthalene is dissolved in 150 ml. of acetic acid and 150 ml. of 48 percent hydrobromic acid, and the mixture is heated at its reflux temperature for two hours. The mixture is diluted with 200 ml. of water and cooled to provide 1-chloro-4-hydroxynaphthalene as a crystalline solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04260547 |
| 出典データセット | uspto-grants-1981_04 |
| ORD ID | ord-70ee28ffc1904d83afb2e39dd9462ea4 |
| 出典メモ | uspto-grants-1981_04 |