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Hydrochloric Acid → H-(D)Ala-Gly-OBzl.hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Diethyl Ether | HCID 3283 | — |
| 反応物 | Boc-(D)Ala-Gly-OBzl | HCID 15567200 | — |
| 溶媒 | 1,4-Dioxane | HCID 31275 | — |
| 生成物 | H-(D)Ala-Gly-OBzl.hydrochloride | HCID 131712174 | — |
反応手順
3.4 g of Boc-(D)Ala-Gly-OBzl are dissolved in 50 ml of dioxane containing HCl and left to stand for one hour. The volume of the solution is reduced under vacuum and an excess of ether added. The precipitated salt is filtered off, dried and used as such for the coupling reaction.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04261888 |
| 出典データセット | uspto-grants-1981_04 |
| ORD ID | ord-bde701a623bf43e4a1e85e704975ba84 |
| 出典メモ | uspto-grants-1981_04 |