Tert-Butylamine → HCID 3055552、化合物
反応式
[CH3:1][C:2]1[S:3][C:4]([CH:7]=[CH:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[O:15][CH2:16][CH:17]2[O:19][CH2:18]2)=[N:5][N:6]=1.[C:20]([NH2:24])([CH3:23])([CH3:22])[CH3:21]>C1(C)C=CC=CC=1>[CH3:1][C:2]1[S:3][C:4]([CH:7]=[CH:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[O:15][CH2:16][CH:17]([OH:19])[CH2:18][NH:24][C:20]([CH3:23])([CH3:22])[CH3:21])=[N:5][N:6]=1参加物
4
実験手順
7 g (0.025 mole) of 2-methyl-5-[2-(2,3-epoxy-propoxy)styryl]-1,3,4-thiadiazole and 2.1 g (0.028 mole) of tert.butylamine are reacted similarly to the Example relating to compound 3. 3.8 g (44% of theory) of yellow crystals, of melting point 110°-112° C., are obtained from toluene.
出典と根拠
- ORDレコード
- ord-aff44ed8ccc149d691127d8b1a36d1e7
- 出典データセット
- uspto-grants-1981_04
- 特許番号
- US04263430
反応ノート
読み込み中…