Hydrochloric Acid → 1-(2,6-Dichlorobenzoyl)-3-(6-(4-chlorophenylthio)-3-pyridinyl)urea, hydrochloride salt

HRID 444469ノート

反応式

HRID 444469 の反応式
[Cl:1][C:2]1[CH:27]=[CH:26][CH:25]=[C:24]([Cl:28])[C:3]=1[C:4]([NH:6][C:7]([NH:9][C:10]1[CH:11]=[N:12][C:13]([S:16][C:17]2[CH:22]=[CH:21][C:20]([Cl:23])=[CH:19][CH:18]=2)=[CH:14][CH:15]=1)=[O:8])=[O:5].Cl>>[ClH:1].[Cl:28][C:24]1[CH:25]=[CH:26][CH:27]=[C:2]([Cl:1])[C:3]=1[C:4]([NH:6][C:7]([NH:9][C:10]1[CH:11]=[N:12][C:13]([S:16][C:17]2[CH:22]=[CH:21][C:20]([Cl:23])=[CH:19][CH:18]=2)=[CH:14][CH:15]=1)=[O:8])=[O:5]

参加物

3

反応物 2

HCID 313Hydrochloric AcidHCID 12912740HCID 12912740、化合物

生成物 1

HCID 1317121961-(2,6-Dichlorobenzoyl)-3-(6-(4-chlorophenylthio)-3-pyridinyl)urea, hydrochloride salt

実験手順

1-(2,6-Dichlorobenzoyl)-3-(6-(4-chlorophenylthio)-3-pyridinyl)urea (2.0 grams) was refluxed in 100 ml. of concentrated HCl (37%) for 4 hours. The reaction mixture was cooled and the product separated by filtration, yield 1.5 grams, m.p., 214°-217° C.

後処理

  1. temperatureThe reaction mixture was cooled
  2. customthe product separated by filtration, yield 1.5 grams, m.p., 214°-217° C.

出典と根拠

ORDレコード
ord-f840c91376c24a519f9115c0519d4b2a
出典データセット
uspto-grants-1981_04
特許番号
US04264605

反応ノート

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