化工社化工社 化学情報印刷レポート · 研究参考用
1,1,1-Trichloroethane → Methacrylic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,1,1-Trichloroethane | HCID 6278 | — |
| 反応物 | 4,4'-Bis(dimethylamino)benzophenone | HCID 7031 | — |
| 反応物 | Glycol monoethyl ether | HCID 8076 | — |
| 反応物 | Leucocrystal Violet | HCID 69048 | — |
| 溶媒 | Methyl Ethyl Ketone | HCID 6569 | — |
| 生成物 | Methacrylic Acid | HCID 4093 | — |
| 生成物 | Methyl Methacrylate | HCID 6658 | — |
反応手順
A solution of 15.0 g of a 9:1 copolymer of methyl methacrylate and methacrylic acid in 50 g of 2-butanone was prepared, and to it was added 15.0 g of Epocryl® 12, 1.2 g of 2-o-chlorophenyl-4,5-diphenylimidazolyl dimer, 0.9 g of Michler's ketone, 0.06 g of Leuco Crystal Violet, 0.30 g of C.I. Solvent Red Dye #109, 16.7 g of methyl chloroform and 150 g of 2-ethoxyethanol. The resulting 13% solids solution was coated onto oriented polyester film substrates using a 0.5 mil (0.00127 cm) doctor knife and dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04264708 |
| 出典データセット | uspto-grants-1981_04 |
| ORD ID | ord-4069bd749e894d57b63f2098bbe96827 |
| 出典メモ | uspto-grants-1981_04 |