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Bis[1-methylimidazole-2-yl methyl]amine → 1-[4-(diethoxymethyl)phenyl]-N,N-bis[(1-methyl-1H-imidazol-2-yl)methyl]methaneamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Bis[1-methylimidazole-2-yl methyl]amine | HCID 358229 | — |
| 反応物 | 4-(Diethoxymethyl)benzaldehyde | HCID 595993 | — |
| 生成物 | 1-[4-(diethoxymethyl)phenyl]-N,N-bis[(1-methyl-1H-imidazol-2-yl)methyl]methaneamine | HCID 67285007 | — |
反応手順
The same procedure as in Example 3 was carried out, except that 1-(1-methyl-1H-imidazol-2-yl)-N-[(1-methyl-1H-imidazol-2-yl)methyl]methaneamine (International Publication WO 2007/058322 pamphlet, Example 58) was used in place of the compound obtained in Example 2, and 4-(diethoxymethyl)benzaldehyde (CAS Registry Number: 81172-89-6) was used in place of isobutylaldehyde in Example 3, the title compound having the following physical properties was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08476290B2 |
| 出典データセット | uspto-grants-2013_07 |
| ORD ID | ord-795a3845d2b34e5a8b5e09388d1342ed |
| 出典メモ | uspto-grants-2013_07 |