Bis[1-methylimidazole-2-yl methyl]amine → 1-[4-(diethoxymethyl)phenyl]-N,N-bis[(1-methyl-1H-imidazol-2-yl)methyl]methaneamine

HRID 445236

反応式

HRID 445236 の反応式
[CH3:1][N:2]1[CH:6]=[CH:5][N:4]=[C:3]1[CH2:7][NH:8][CH2:9][C:10]1[N:11]([CH3:15])[CH:12]=[CH:13][N:14]=1.[CH2:16]([O:18][CH:19]([O:28][CH2:29][CH3:30])[C:20]1[CH:27]=[CH:26][C:23]([CH:24]=O)=[CH:22][CH:21]=1)[CH3:17]>>[CH2:29]([O:28][CH:19]([O:18][CH2:16][CH3:17])[C:20]1[CH:27]=[CH:26][C:23]([CH2:24][N:8]([CH2:7][C:3]2[N:2]([CH3:1])[CH:6]=[CH:5][N:4]=2)[CH2:9][C:10]2[N:11]([CH3:15])[CH:12]=[CH:13][N:14]=2)=[CH:22][CH:21]=1)[CH3:30]

参加物

3

反応物 2

HCID 358229Bis[1-methylimidazole-2-yl methyl]amineHCID 5959934-(Diethoxymethyl)benzaldehyde

生成物 1

HCID 672850071-[4-(diethoxymethyl)phenyl]-N,N-bis[(1-methyl-1H-imidazol-2-yl)methyl]methaneamine

実験手順

The same procedure as in Example 3 was carried out, except that 1-(1-methyl-1H-imidazol-2-yl)-N-[(1-methyl-1H-imidazol-2-yl)methyl]methaneamine (International Publication WO 2007/058322 pamphlet, Example 58) was used in place of the compound obtained in Example 2, and 4-(diethoxymethyl)benzaldehyde (CAS Registry Number: 81172-89-6) was used in place of isobutylaldehyde in Example 3, the title compound having the following physical properties was obtained.

出典と根拠

ORDレコード
ord-795a3845d2b34e5a8b5e09388d1342ed
出典データセット
uspto-grants-2013_07
特許番号
US08476290B2

関連ノート

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