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4,4-Dimethylcyclohexen-1-ylboronic acid → 5-[4-Amino-3-(4,4-dimethyl-cyclohex-1-enyl)-phenyl]-1,3-dimethyl-tetrahydro-pyrimidin-2-ylidene-cyanamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4,4-Dimethylcyclohexen-1-ylboronic acid | HCID 44119555 | — |
| 反応物 | HCID 86615904 | HCID 86615904 | — |
| 生成物 | 5-[4-Amino-3-(4,4-dimethyl-cyclohex-1-enyl)-phenyl]-1,3-dimethyl-tetrahydro-pyrimidin-2-ylidene-cyanamide | HCID 86615903 | — |
反応手順
The title compound was prepared according to the Suzuki coupling procedure of Example 3, step (a), using 4,4-dimethyl-cyclohex-1-enyl boronic acid and 5-(4-amino-3-bromo-phenyl)-1,3-dimethyl-tetrahydro-pyrimidin-2-ylidene-cyanamide Mass spectrum (ESI, m/z): Calcd. for C21H29N5, 352.2 (M+H), found 352.4
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08481564B2 |
| 出典データセット | uspto-grants-2013_07 |
| ORD ID | ord-d960ffbf11d844e7afe5ed79ce29553c |
| 出典メモ | uspto-grants-2013_07 |