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Ethyl 1-aminocyclohexane-1-carboxylate hydrochloride → HCID 57672866、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 1-aminocyclohexane-1-carboxylate hydrochloride | HCID 11241228 | — |
| 反応物 | 4-(4-Propylpiperazin-1-yl)benzoic acid hydrochloride | HCID 67181841 | — |
| 生成物 | HCID 57672866 | HCID 57672866 | 65% |
反応手順
741 mg (3.57 mmol) of 1-aminocyclohexanecarboxylic acid ethyl ester hydrochloride was used instead of 1-aminocyclohexanecarboxylic acid methyl ester hydrochloride, and 1.00 g (3.57 mmol) of 4-(4-propylpiperazin-1-yl)benzoic acid hydrochloride was used instead of 3-furancarboxylic acid in the process according to Reference Example 15 to obtain 928 mg (65%) of the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08481725B2 |
| 出典データセット | uspto-grants-2013_07 |
| ORD ID | ord-16c1c33e765c4754afa8c16d55cafadf |
| 出典メモ | uspto-grants-2013_07 |