化工社化工社 化学情報印刷レポート · 研究参考用
Aminoacetaldehyde dimethyl acetal → 7-Bromo-6-methylisoquinoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aminoacetaldehyde dimethyl acetal | HCID 89728 | — |
| 反応物 | 3-Bromo-4-methylbenzaldehyde | HCID 816765 | — |
| 生成物 | 7-Bromo-6-methylisoquinoline | HCID 59496589 | — |
反応手順
This compound was prepared by using procedures analogous to those described for the synthesis of Example 75, Step 1 starting from 3-bromo-4-methylbenzaldehyde (Aldrich, Cat. #4017458) and. aminoacetaldehyde dimethyl acetal. Analytic LCMS (M+H)+: m/z=221.95/223.95.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08481732B2 |
| 出典データセット | uspto-grants-2013_07 |
| ORD ID | ord-66fcfe8a5a6d463f9b6baa757d41bd3f |
| 出典メモ | uspto-grants-2013_07 |